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Topic: MDP2P

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In the News (Wed 20 Jun 18)

  Encyclopedia: Ecstasy (drug)   (Site not responding. Last check: 2007-11-05)
MDMA is synthesized from MDP2P through a chemical reaction known as reductive amination.
MDP2P is a phenylacetone that has the IUPAC name 3,4-methylenedioxy phenyl-2-propanone.
Reductive amination is a type of amination reaction which involves the conversion of a carbonyl group to an amine.
www.nationmaster.com /encyclopedia/Ecstasy-%28drug%29   (8168 words)

 the Lycaeum - Alchemist's Den   (Site not responding. Last check: 2007-11-05)
In Reply to: High yield prep of MDP2P from Piperonal posted by rhodium@nym.lycaeum.org on October 02, 1997 at 12:55:30:
It details a high yield > synthesis of MDP2P from piperonal.
I always said trash pickin' was the way to go..
www.lycaeum.org /forums/alchemy/Messages/342.html   (211 words)

 DanceSafe E-Board: How MDMA is made   (Site not responding. Last check: 2007-11-05)
While this may sound rather straightforward, safrole, MDP2P and methylamine are are watched/controlled chemicals which are extremely difficult, if not impossible for the average clandestine chemist to acquire and generally must be first synthesized (or in the case of safrole, extracted) from other, more readily available sources.
In this reaction, safrole in the presence of Palladium Chloride (PdCl2) and benzoquinone is converted to its ketone, MDP2P.
Once both MDP2P and methylamine have been synthesized, these two compounds are reacted in the presence of Al/Hg to form MDMA freebase.
www.dancesafe.org /ubbthreads/showflat.php?Cat=0&Number=131215&an=0&page=0   (586 words)

 the Lycaeum - Alchemist's Den   (Site not responding. Last check: 2007-11-05)
Preparation of 1-(3,4-methylenedioxyphenyl)-2-nitropropene 15g of piperonal was dissolved in 40ml of MeOH under stirring in a 250ml Erlenmeyer flask.
This nitrostyrene should be used within a week, or stored in the cold, as the color fades to a slight orange over a couple of weeks in room temperature, which is a sign of decomposition.
Preparation of 1-(3,4-Methylenedioxyphenyl)-2-propanone (MDP2P) 25g (0.12 mols) 1-(3,4-methylenedioxyphenyl)-2-nitropropene was dissolved in 350ml methanol in a 500ml Erlenmeyer flask situated on a magnetic stirrer, and chilled to -10°C with an ice/salt bath.
www.lycaeum.org /forums/alchemy/Messages/339.html   (866 words)

 MDMA / Ecstasy : Utopian Pharmacology
MDP2P (3,4-methylenedioxyphenyl-2-propanone) is a commercial product used by the flavouring and fragrance industry.
Otherwise, MDMA must be synthesized from piperonal, isosafrole, or safrole.
Typically, safrole or isosafrole are first converted to MDP2P.
www.mdma.net /index.html   (16378 words)

 Production - Joint Assessment of MDMA Trafficking Trends   (Site not responding. Last check: 2007-11-05)
Although safrole (the primary constituent of sassafras oil), isosafrole, and piperonal are the three primary MDMA precursor chemicals, many production groups are able to acquire MDP2P (3,4-methylenedioxyphenyl-2-propanone), and produce MDMA in a simple conversion process rather than starting the process with one of the precursor chemicals.
MDP2P is a commercial product made overseas and imported for use by the flavoring and fragrance industry.
Conversion of safrole to MDP2P using sulfuric acid, sodium hydroxide, and solvents; conversion from isosafrole using hydrogen peroxide and formic acid results in reduced yields
www.usdoj.gov /ndic/pubs/642/product.htm   (1257 words)

 Synthesis of Quinones and Hydroquinones
Methylamine is no longer a stumbling block in the aluminum amalgam reductive alkylation method of producing MDMA as this procedure produces this impossible to obtain and fickle to make material, in situ, during the reductive alkylation of MDP2P to MDMA from very common nitromethane.
An alcoholic solution of nitromethane and MDP2P is dripped into a mass of amalgamated aluminum immersed in alcohol first reducing the nitromethane to methylamine, allowing the Schiff base of the amine and ketone to form which is further reduced to the desired MDMA.
After about 5-10 minutes the bubbling should be sufficient and you may start adding the methanolic mixture of nitromethane and MDP2P drop by drop from the separatory funnel.
designer-drugs.com /pte/   (1098 words)

 Q3_2004   (Site not responding. Last check: 2007-11-05)
The precursor substance found, known as MDP2P, was enough to produce 21.2 million doses of ecstasy - nearly 10 times more than the last record seizure of ecstasy in 2003.
But when it was discovered that 66 of the soy sauce jugs contained about 1,800 kg of the precursor substance, RCMP were immediately contacted to place the shipment under surveillance.
What followed was a month-long investigation in which RCMP tracked the delivery of MDP2P to a Vancouver storage facility.
www.yorku.ca /nathanson/CurrentEvents/July-Sept04.htm   (8872 words)

 Irreality Cut Up Library: Chemical Transcendence Mix - Iki   (Site not responding. Last check: 2007-11-05)
Rxn: Safrole may be re-dissolved in dilute hydrochloric crystal of your product on the occasionally during the heating and push of the vapors rises to ~85°C. The times.
Abstract: Reduction of the hydroxyl 20g of urea, and place the plus approximately 25°C is the temp the solution, and filtering off the We are removing methylal, and methylformate Reaction contents to yield pure MDP2P weekends or in a straight shot.
Step 6: Evaporation Finally, pour to use zincorganic compounds instead (discussed was maintained for four hours at slowly.) The ketone oil is a 3000 coulombs have passed through the the ingot, and wth the piece distill this with the stirbar in grey sludge will settle to the mixture of 100mL 'Dry' IPA and concentration.
www.iki.org.uk /index.php/Irreality_Cut_Up_Library:_Chemical_Transcendence_Mix   (11975 words)

 DEA Resources, Microgram, January 2003
The synthetic route to MDMA involved reductive amination of 3,4-methylenedioxyphenylacetone (MDP2P or PMK) with methylamine and sodium borohydride; the hydrochloride salt was produced by gassing an acetone solution of the free base with commercial hydrochloric acid gas.
Small amounts of MDA were also produced by contamination of the amphetamine syntheses with MDP2P (and MDA was therefore identified in some of the resulting tablets).
The concomitant seizure of the tabletting operation (and all its associated tablet dies) indicated that the operation was producing tablets with 23 different monograms.
www.usdoj.gov /dea/programs/forensicsci/microgram/mg0103/mg0103.html   (7232 words)

Phenyl acetone is used as an intermediate to produce sympathomimetic amines such as phenbenzamine, phenyl isopropyl amine, amphetamine, prenylamine, pargyline and estramustine.
Phenylacetone is called MDP2P (3,4-methylenedioxy phenyl-2-propanone) which is used in the clandestine synthesis of MDMA (3,4-methylenedioxymethamphetamine), commonly known as ecstasy.
Phenylacetone shipment is available only to the importer who has import licence issued by Government.
www.chemicalland21.com /arokorhi/specialtychem/finechem/PHENYLACETONE.htm   (429 words)

 [No title]   (Site not responding. Last check: 2007-11-05)
\end{itemize} The Atlas group leads the MDP2P (Massive data management in peer-to-peer systems) project funded by the ACI ``Masses of Data'' of the French ministry of research.
The MDP2P project is scheduled for 3 years (2003-2006) and involves three other INRIA groups: Paris and Texmex in Rennes, and Gemo in Orsay.
B\'ezivin is a member of the ALP GDR and is involved in the French object research community, through the two main conferences Objet'XX and OCM'XX.
www.sunsite.org.uk /sites/ftp.inria.fr/INRIA/publication/Theses/RAWEB-SV/atlas/atlas2003.tex   (4669 words)

 What's With All the Dutch Ecstasy? - Why it's not made in the USA. By Brendan I. Koerner   (Site not responding. Last check: 2007-11-05)
The problem in the United States is that law enforcement tends to monitor the purchase of the precursor chemicals required to synthesize ecstasy.
Chemical-supply companies often tip off the Drug Enforcement Administration when a customer purchases, say, an unusually large amount of isosafrole or MDP2P, two critical ingredients in ecstasy recipes.
DEA agents sometimes pose as chemical salesmen in order to bust suspected ecstasy cooks.
slate.msn.com /id/2098128   (625 words)

 ghb synthesis procedure - see information on ghb synthesis procedure provided by Steroid Encyclopaedia
Mix butyrolactone and NaOH in pyrex dish, and add water.
Procedure for the oxidation of isosafrole to MDP2P using Oxone...
Lab procedure for the synthesis of GHB: Please follow common Lab Safety procedures.
www.steroid-encyclopaedia.com /36/ghb-synthesis-procedure.html   (559 words)

 Irreality: Alchemy - MDMA - Iki   (Site not responding. Last check: 2007-11-05)
There is some prep-work that can be done ahead of time, or while you're distilling.
When it was settled (notice that the layer now is a different color) the aqueous layer was poured off again into another jar where it was washed again with another 100mL portion of fresh DCM = 2x100mL washes.
Distillation: of Reaction contents to yield pure MDP2P Pour the DCM/Organic layer into your CLEAN 500mL RBFlask.
www.iki.org.uk /index.php/Irreality:_Alchemy_-_MDMA   (4420 words)

 The Seattle Times: Local News: Seattle arts group names managing director
Four Canadians have been charged in the case that also led to the seizure of nearly 1,600 pounds of marijuana and about $610,000 in cash, the Royal Canadian Mounted Police said.
Border guards became suspicious about a shipping container that arrived in Vancouver in late July and found that 66 cartons in a 400-carton shipment of soy sauce actually contained a yellow liquid later identified as the chemical MDP2P.
Police did not put a dollar value on the seizure, but estimated the chemical was enough to help produce 21.2 million doses of ecstasy.
seattletimes.nwsource.com /html/localnews/2002014724_dige25m.html   (591 words)

 Mailgate: rec.drugs.chemistry: Re: Difference between Ephedrine and Pseudo Ephedrine?   (Site not responding. Last check: 2007-11-05)
These aren't : readily available at all, and must be handled under rigorously dry and : air-free conditions.
This means reactions done in a dry nitrogen purged : glovebox using specially dried solvents, none of which is needed when going : via MDP2P.
Even going via this (albeit rather clever) route, you will still : end up with racemic MDMA.
mailgate.supereva.it /rec/rec.drugs.chemistry/msg02884.html   (349 words)

 CBC British Columbia - Four charged in major drug bust   (Site not responding. Last check: 2007-11-05)
At the Delta Port, police also seized nearly 1,800 kilograms of a substance used to manufacture ecstasy.
The chemical MDP2P was hidden in containers labelled as soy sauce aboard a ship – and was enough to make more than 21.2 million doses of the drug.
Li, Feng, Tsang and Ma have all been charged with conspiracy to produce ecstasy.
vancouver.cbc.ca /regional/servlet/View?filename=bc_bust20040824   (231 words)

 Reductive Amination of MDP2P with Al/Hg + Nitromethane
Reductive Amination of MDP2P with Al/Hg + Nitromethane
Since the appearance of Ritter's writeup of this method in Total Synthesis II, much discussion has taken place about it but, it has sometimes seemed, little has been clarified.
While Charlie Brown and Linus were away at school, Snoopy decided to have some fun.
designer-drugs.com /pte/   (3314 words)

 [No title]
Subject: MDP2P directly from safrole Date: 8 Apr 1998 16:24:51 GMT From: Rhodium
Newsgroup: alt.drugs.chemistry Found an interesting MDP2P synthesis the other day in this patent.
8.50g (47.75 mmol) of piperonylmethylketone (MDP2P) was thus obtained and 8.70g (53.7 mmol) of unreacted safrole was recovered; selectivity to the ketone, with respect to the converted safrole, was 72% [End of transmission]
www.intellicandy.com /oldschool/chemcandy/mdp2p.patent.txt   (923 words)

 Chemical profiling of 3,4-methylenedioxymethamphetamine (MDMA) tablets seized in Hong Kong. Cheng WC, Poon NL, Chan MF ...   (Site not responding. Last check: 2007-11-05)
The impurities detected in the MDMA tablets also served as excellent chemical markers from which plausible synthetic route(s) of the MDMA were inferred.
Our study revealed that 3,4-methylenedioxyphenyl-2-propanone (MDP2P), 3,4-methylenedioxyphenyl-2-propanol (MDP), 3,4-methylenedioxy-N-methylbenzylamine (MDB), piperonal and N-formyl-3,4-methylenedioxymethamphetamine (N-formyl-MDMA) were the most common impurities detected in MDMA tablets seized in Hong Kong.
The finding of the phosphate salt of MDMA is intriguing.
www.astm.org /jforensicsci/PAGES/4334.htm   (272 words)

 cannabiscafe - De donde viene naturalmente el ectasy?   (Site not responding. Last check: 2007-11-05)
La producción clandestina es más sencilla si se parte del MDP2P (3,4-methylenedioxyphenyl-2-propanone), un producto comercial usado como saborizante y en la industria del perfume.
Los que tienen acceso al MDP2P pueden fabricar MDMA mediante un proceso simple de conversión.
Típicamente, el safrol o el isosafrol se convierten a MDP2P.
www.cannabiscafe.net /foros/showthread.php?s=&threadid=29018   (384 words)

 Rhodium a DEA front? - Shroomery Message Board
If you go to a public library for anything other than the absolute grade school basics, you shouldn't be trying to deal with the legalities involving purchasing things needed to put the knowledge you seek to use anyways.
From someone who's condescension doesn't get in the way of their message:
I know why the sites are important, and it's primarily due to the concentration of relevant info.
www.shroomery.org /forums/showflat.php?Cat=0&Board=safety&Number=3440890&page=0&fpart=3   (1057 words)

 sludge it yields is too thin   (Site not responding. Last check: 2007-11-05)
Osmium's variation on the Al/Hg reductive amination of MDP2P.
My first experiments were performed according to Shulgin's procedure with P2P and MDP2P.
In reduction using thin Al foil (huge surface...
all-your-finances.com /articles/380/sludge-it-yields-is-too-thin.html   (390 words)

 Review - More News September 2, 2004
That charge relates to the discovery of the ecstasy precursor chemical, which was found July 21 in a shipment that purported to contain 400 cartons of soy sauce and 450 cartons of rice noodles.
Canada Border Services Agency examined the shipment and found 66 cartons that were labelled as soy sauce but actually contained jugs filled with a suspicious yellow liquid, which turned out to be a controlled substance known as MDP2P.
The police were called in, and during the course of a month-long investigation delivered the shipment from Delta Port to a Vancouver storage facility.
www.yourlibrary.ca /community/richmondreview/archive/RR20040902/morenews.html   (7905 words)

 MDMA Synthesis for the First Time Chemist
Distillation: of Reaction contents to yield pure MDP2P
Rxn: MDP2P -(Al/Hg Amalgam (MeAm.HCl) -> MDMA oil
Pour the DCM/Organic layer into your CLEAN 500mL RBFlask.
www.angelfire.com /ego/mdma/mdma.html   (4678 words)

 Slashdot | Australian Scramjet Launched
Apparently it didn't do what it should have after all.
by mdp2p (533221) on Wednesday October 31, @01:59AM (#2501487)
My dad went to the USA and was told 'You speak good english for an Australian' and Isn't Australia just over the river.
slashdot.org /articles/01/10/30/1258219.shtml?tid=126   (4010 words)

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