| | Patent 4806638: Neutralization of reaction mixtures obtained by Beckman rearrangement of cyclohexanone oxime (Site not responding. Last check: 2007-11-05) |
 | | In this procedure, the neutralization may be effected with gaseous ammonia or ammonia in aqueous solution or together with ammonium sulfate mother liquor, and the ammonia can be combined with the ammonium sulfate solution either upstream of the neutralization stage or directly in the neutralization stage. |
 | | In the neutralization with itroduction of gaseous ammonia through a plurality of nozzel orifices, it has been found that these orifices become blocked within a short time, and uniform feed of ammonia into the medium to be neutralized, and hence satisfactory neutralization of the said medium, are not ensured. |
 | | It is an object of the present invention to provide a process for the neutralization of reaction mixtures from the Beckmann rearrangement reaction, in which gaseous ammonia is fed in during the neutralization without difficulties and uniform neutralization of the reaction mixture is ensured. |
| www.freepatentsonline.com /4806638.html (1988 words) |