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| | Microwave-Assisted Extraction and Accelerated Solvent Extraction with Ethyl Acetate-Cyclohexane before Determination of ... (Site not responding. Last check: 2007-09-26) |
 | | Focused open-vessel microwave-assisted extraction (FOV—MAE), closed-vessel microwave-assisted extraction (CV—MAE), and accelerated solvent extraction (ASE) were used for extraction before determination of organochlorine compounds (polychlorinated biphenyls, DDT, toxaphene, chlordane, hexachlorobenzene, hexachlorocyclohexanes, and dieldrin) in cod liver and fish fillets. |
 | | Extractions were performed with the solvent mixture ethyl acetate—cyclohexane (1 + 1, v/v), which allowed direct use of gel-permeation chromatography without solvent exchange. |
 | | For this reason, the extraction procedure for wet fish tissue required 2 extraction steps: the first for manual removal of coextracted water, and the second for quantitative extraction of the organochlorine compounds with the pure solvent. |
| www.aoac.org /pubs/JOURNAL/2000/Nov_Dec/Microwave_Assisted.htm (257 words) |
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